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Through precise, detailed coverage of the principles, equipment, and techniques involved in separation science, this combination of laboratory manual, textbook and reference source gives readers a working knowledge of an impressive array of separation methods. In 42 chapters, it explores all major categories of separation, including those involving phase changes, extraction, chromatography, ion-exchange resins, electric fields, flotation, membranes, and miscellaneous techniques.

Table of contents

	Introduction	1
	Separations Involving Phase Changes
1	Volatilization	5
2	Zone Melting	13
3	Distillation: General Information	21
4	Azeotropic and Extractive Distillations	43
5	Steam and Immiscible Solvents Distillation	49
6	Vacuum Distillation	57
7	Molecular Distillation and Sublimation	71
8	Lyophilization (Freeze Drying)	85
	Separations Involving Extraction
9	Extraction: General Concepts	93
10	Continuous Extraction	107
11	Countercurrent (Extraction) Chromatography: The Ito Coil-Planet Centrifugal Extractor	117
12	Solid Phase Extraction	129
13	Supercritical Fluid Extraction	137
	Separations Involving Chromatography
14	Chromatography: General Theory	149
15	Displacement and Multiple Column Partition Chromatography	155
16	Affinity Chromatography	165
17	Size Exclusion Chromatography (Gel Filtration; Gel Permeation)	171
18	Flash Chromatography	179
19	High Performance Liquid Chromatography (HPLC)	183
20	Gas-Liquid Chromatography (GLC)	211
21	Paper Chromatography	249
22	Thin Layer Chromatography	255
	Separations Involving Ion Exchange Resins
23	Ion Exchange	269
24	Ion Chromatography	277
25	Ion Retardation, Ion Exclusion, and Ligand Exchange	289
	Separations Involving Electric Fields
26	Electrodeposition	299
27	Electrophoresis - General	315
28	Immunoelectrophoresis	339
29	Polyacrylamide Gel Disc Electrophoresis	345
30	Ion Focusing, SDS, and Two-Dimensional Electrophoresis	351
31	Capillary Zone Electrophoresis	359
32	Field Flow Fractionation	371
	Separations Involving Flotation
33	Purge and Trap and Dynamic Headspace Analysis	385
34	Foam Fractionation, Gas-, and Liquid-Assisted Flotation	395
	Separations Involving Membranes
35	Osmosis and Reverse Osmosis	413
36	Dialysis and Electrodialysis	423
37	Filtering and Sieving	431
	Separations Involving Miscellaneous Techniques
38	Density Gradients	449
39	Centrifugation	455
40	Masking and Sequestering Agents	469
41	Solubility	473
42	Gas Analysis by Portable Orsat	489
App. A	Experiments	499
	App. B: Answers to the Review Questions	711
	Index	747